ANALYSIS TECHNIQUES
LABORATORY INSTRUMENTATION
1. AE and FTIR Spectroscopy
The Atomic Emission (AE) Spectrometer determines the level of
wear metals and contaminants in used lubricating oils and hydraulic fluids.
The Fourier Transform Infrared (FTIR) Spectrometer is used to identify organic
materials by measuring the absorption of various infrared light wavelengths by
the material of interest.
2. Viscometry
The kinematic viscosity of a fluid is determined by measuring
the time for a volume of liquid to flow under gravity through a calibrated
Zeitfuchs cross arm glass capillary tube suspended in a water or oil bath,
maintained at a constant temperature of 100C or 40C.
3. Moisture Titration
The volumetric water content of used lubricating oil is
determined by Karl Fischer titration.
4. Acid and Base Titration
The Automatic Potentiometric Titrator (Karl Fischer) is used
for the determination of the concentration of a liquid or solid by titration
method. This allows for the measurement of acidic and basic constituents of
the fluid. From this it can be determined whether the additive system is still
capable of neutralizing acid residues.
5. Reserve Alkalinity Titration
The Automatic Potentiometric Titrator is also used for the
determination of the effectiveness and remaining life of a coolant, based on
additive degradation and contamination.
6. ISO Cleanliness
A fluid contamination comparitor is used to estimate the
amount and type of solid contamination in a hydraulic oil or lubricating oil.
ISO Cleanliness Codes are given using the revised ISO 4406 (FDIS) procedure
for reporting fluid cleanliness measurements resulting from APC's calibrated
with the new NIST traceable method.
7. LMOA Pentane Insolubles
A filtration procedure, in accordance with the LMOA Fuels,
Lubricants and Environmental Committee Standard Insolubles Test Method
Revision 3, is used for the determination of coagulated pentane insolubles in
used lubricating oils.
THE OIL-PLUS™ SYSTEM
For an overview of the automated machinery oil analysis program
click here.
EXPERT SYSTEM
To review the purpose and objectives of trend analysis
click here.
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